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Synthesis, structure and magnetic properties of iron (II), cobalt (II) and nickel (II) complexes of 2,6-bis(pyrazol-3-yl)pyridine and paramagnetic counterions by Eugenio Coronado; Mari Carmen Giménez-López; Carlos Gimenez-Saiz; José M. Martı́nez-Agudo; Francisco M. Romero is a Chemistry article available to read on EtoBox.
What is Synthesis, structure and magnetic properties of iron (II), cobalt (II) and nickel (II) complexes of 2,6-bis(pyrazol-3-yl)pyridine and paramagnetic counterions about?
Iron (II), cobalt (II) and nickel (II) complexes of 2,6-bis(pyrazol-3-yl)pyridine (bpp) with [Cr(C 2 O 4 ) 3 ] 3( have been prepared. They were characterised by single-crystal X-ray diffraction, magnetic susceptibility measurements and thermal gravimetric analyses. All three compounds are isostructural and they are formed by isolated [M II (bpp) 2 ] 2' and [Cr(C 2 O 4 ) 3 ] 3( complexes and free ClO 4 ( . As expected, only the salt [Fe(bpp) 2 ] 2 [Cr(C 2 O 4 ) 3 ]ClO 4 ×/5H 2 O shows a thermal spin transition with transition temperature (T 1/2 ) around 375 K that is correlated to the loss of water molecules.
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- Author
- Eugenio Coronado; Mari Carmen Giménez-López; Carlos Gimenez-Saiz; José M. Martı́nez-Agudo; Francisco M. Romero
- Publisher
- Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0277-5387)
- Published
- 2003
- Language
- EN
- Field
- Chemistry (Physical Sciences)