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Lignin-based carbon dots as high-performance support of Pt single atoms for photocatalytic H2 evolution 1 1 Introduction 1 2 Experimental section 2 2.1 Materials 2 2.2 Synthesis of the samples 2 2.2.1 Synthesis of NLCDs 2 2.2.2 Synthesis of Pt-NLCDs 2 2.2.3 Synthesis of CdS nanorods 2 2.2.4 Synthesis of Pt-NLCDs@CdS 2 2.3 Characterizations 2 2.4 Theoretical calculations 3 2.5 Photoelectrochemical measurement 3 2.6 PHE performance tests 3 3 Results and discussion 3 3.1 Characterizations of NLCDs and Pt-NLCDs 3 3.2 Simulation of Pt atoms on N-doped LCDs 5 3.3 Characterization of Pt-NLCDs@CdS 6 3.4 Photocatalytic H2 evolution performance 7 3.5 Optical properties and photoelectrochemical analyses 9 3.6 Photocatalytic mechanism 11 4 Conclusion 11 CRediT authorship contribution statement 12 Declaration of Competing Interest 12 Acknowledgment 12 Appendix A Supplementary data 12 References 12
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