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Characterization of the unsymmetrical trimer of indole‐5‐carboxylic acid by proton NMR spectroscopy by J. G. Mackintosh; A. R. Mount; D. Reed is a Chemistry article available to read on EtoBox.
What is Characterization of the unsymmetrical trimer of indole‐5‐carboxylic acid by proton NMR spectroscopy about?
## Abstract Indole‐5‐carboxylic acid trimer, a major product formed during the electro‐polymerization of indole‐5 carboxylic acid, was characterized by ^1^H NMR spectros‐copy, and a wide range of one‐ and two‐dimensional NMR techniques were employed to allow full analysis of the ^1^H spectrum. Homonuclear NOE experiments were carried out in different solvents and at different temperatures, owing to the unusual observation of negative enhancements in some experiments. This was shown to be due to the slow tumbling rate of the molecule.
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- Author
- J. G. Mackintosh; A. R. Mount; D. Reed
- Publisher
- John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Inc.; John Wiley and Sons Ltd; Wiley (ISSN 0749-1581)
- Published
- 1994
- Language
- EN
- Field
- Chemistry (Physical Sciences)