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This document describes a study examining the oxidation of aliphatic amines to nitroalkanes using meta-chloroperbenzoic acid (m-CPBA). The researchers found that direct oxidation of amines with m-CPBA in halocarbon solvents gave mixtures. However, oxidation in dichloromethane at 0°C for 30 minutes followed by warming to room temperature for 16 hours provided good to excellent yields of the corresponding nitroalkanes for various primary and secondary amines tested. This method provides a general synthesis of

Author

Sunny Chosa

Language

EN