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The document details the synthesis of chromium (II) acetate, which features a Cr-Cr quadruple bond, achieved by reducing CrCl3·6H2O in a low oxygen environment using zinc and hydrochloric acid. The experiment yielded a 16.2% success rate, with careful attention needed to prevent oxidation of Cr2+ to Cr3+. The study highlights the importance of maintaining an inert atmosphere and the role of bidentate ligands in facilitating the formation of the quadruple bond.
- Author
- JP
- Language
- EN