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RSM optimization studies for cadmium ions adsorption onto pristine and acid-modified kaolinite clay 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Preparation of acid-modified kaolinite clay adsorbent 2 2.3 Characterization of acid-modified kaolinite clay adsorbents 2 2.4 Equilibrium batch adsorption studies 3 2.5 Optimization of Cd(II) ions adsorption by acid-modified clay 3 2.6 Point of zero charge (pHpzc) 3 2.7 Isotherm study 3 2.8 Kinetic study 4 2.9 Non-linear regression method 5 2.10 Error analysis 5 2.11 Thermodynamic study 5 2.12 Desorption study 6 3 Results and discussion 6 3.1 Adsorbent characterizations 6 3.2 Response surface methodology for Cd ions removal by PKC and AMKC 6 3.3 Effect of parameters as response surface plots 10 3.3.1 Response surface plots for Cd2+ uptake removal by AMKC 10 3.3.2 Response surface plots for Cd2+ ions uptake removal by PKC 11 3.4 Process optimization 11 3.5 Point of zero charge determination 11 3.6 Effect of pH 11 3.7 Adsorption isotherms study 11 3.8 Adsorption kinetics study 12 3.9 Adsorption thermodynamics study 13 3.10 Desorption study 14 4 Conclusions 15 Author contribution statement 16 Data availability statement 16

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UND

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nonfiction