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## 1. General Information Reactions were carried out under a dry argon atmosphere. Anhydrous N,N-dimethylformamide (DMF), dimethyl sulfoxide (DMSO), N,N-dimethylacetamide (DMA), cyclopentyl methyl ether (CPME), 2-methyltetrahydrofuran (2-MeTHF), tert-butanol ( t BuOH), toluene and dimethoxymethane (DME) were all purchased from J&K Chemicals and directly used without further purification. Unless otherwise stated, reagents, including all alcohols, were commercially available and used as purchased without further purification. Chemicals were purchased from J&K Chemicals, Adamas-beta, Macklin Reagent, Energy Chemicals, Aladdin, JiuDing Chemicals or Bide Pharmatech Ltd. The progress of the reactions was monitored by thin-layer chromatography using Whatman Partisil K6F 250 μm precoated 60 Å silica gel plates and visualized by short-wave ultraviolet light as well as by treatment with iodine. Flash chromatography was performed with silica gel (300-400 mesh). The NMR spectra were obtained using Brüker 400 MHz or 600 MHz Fourier-transform NMR spectrometer. Chemical shifts are reported in units of parts per million (ppm) downfield from tetramethylsilane (TMS), and all coupling constants are r

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction