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Magnetic Resonance Imaging of Catalysts and Catalytic Processes 1 Introduction 2 Introduction to MRI Techniques 5 Principles of MR Measurements 5 Obtaining an Image 5 Nuclear Spin Relaxation Times 7 The k-Space Raster 10 Measurement of Diffusion, Dispersion, and Flow 13 Phase-Encoding Methods 13 Time-of-Flight Methods 18 Rapid Image Acquisition 19 Contrast Mechanisms 19 Obtaining Chemical Information 19 Relaxation and Transport Contrast 22 Temperature 24 Recent Developments 24 Gas-Phase MR 24 Fast Data Acquisition 25 Imaging Individual Catalyst Pellets 32 Structure-Transport Relationships 32 Catalyst Preparation 34 Liquid Redistribution During Reaction 35 Coke Deposition 37 Hydrodynamics in Reactors 38 Single-Phase Flow 39 High Spatial Resolution of Fluid Flow in Fixed-Bed Reactors 39 Imaging Unsteady-State Flows in Fixed-Bed Reactors 43 Two-Phase Flow in Fixed-Bed Reactors 45 Holdup and Wetting in Trickle Flow 45 The Trickle Flow to Pulse Flow Transition 50 Two-Phase Flow in Ceramic Monoliths 52 Fluidized Beds 57 Imaging of Reactions In Situ 59 Single-Phase Reactions in Fixed Beds 60 An Esterification Reaction 60 Probing Selectivity with 13C Imaging 65 Two-Phase Flow and Reaction

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Elsevier