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Resolution effects of organic additives on the MEKC enantiomeric separations of tri aza aromatic ligand compounds of iron(II) by Marjorie M. See; Said Elshihabi; John A. Burke Jr.; Michelle M. Bushey is a Engineering article available to read on EtoBox.

What is Resolution effects of organic additives on the MEKC enantiomeric separations of tri aza aromatic ligand compounds of iron(II) about?

We have utilized micellar electrokinetic chromatography with sodium deoxycholate micelles to separate the enantiomers of bis(S-((pyridine-2methylene)amino)quinoline)iron(II) hexafluorophosphate, Fe(PMAQ),(PF,),, bis(8-((pyridine-2-methylene)amino)lepidine iron(I1) hexafluorophosphate, Fe(PMAL),(PF,),, and bis(1-(2-pyridinyl)ethylidine)-8-aminoquinoline iron(I1) hexafluorophosphate, Fe(PEAQ),(PF,),. The influence of 13 water miscible organic additives on the resolution of each pair of enantiomers was investigated. Significant changes in resolution are seen depending upon the particular organic additive used in the separation buffer. In addition, the effects of acetone concentration on the resolution of these enantiomers in bile salt solution was investigated. Resolution for all three pairs of enantiomers is maximized in a buffer solution containing 15% acetone.

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Author

Marjorie M. See; Said Elshihabi; John A. Burke Jr.; Michelle M. Bushey

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Ltd.; Wiley (ISSN 1040-7685)

Published

1995

Language

EN

Field

Engineering (Physical Sciences)