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Facile fabrication of ZnO decorated ZnFe-layered double hydroxides @ biochar nanocomposites for synergistic photodegradatio ... 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Facile synthesis of ZnO/ZnFe-LDH@BC nanocomposites 2 2.3 Characterization methods 2 2.4 Evaluation of visible light photocatalytic performance 2 3 Results and discussion 3 3.1 Characterizations 3 3.1.1 Structure and morphology analyses 3 3.1.2 Optical and electrochemical properties 4 3.2 Synergistic photocatalytic performance of ZnO/ZnFe-LDH and BC 5 3.3 Practicability of ZnO/[email protected] 6 3.3.1 Effect of the initial pH 6 3.3.2 Effect of inorganic anions 7 3.3.3 Performance in natural water 7 3.3.4 Stability and recyclability of ZnO/[email protected] 8 3.4 Possible photocatalytic mechanism 9 3.5 The possible degradation pathway of TC and toxicity analysis 10 4 Conclusions 10 CRediT authorship contribution statement 11 Declaration of Competing Interest 11 Acknowledgements 11 Appendix A Supplementary data 11 References 11

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UND

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nonfiction