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Peroxydisulfate production in␣situ by blue titania nanotube array electrode for tetracycline degradation in groundwater: Performance and mechanism 1 1 Introduction 1 2 Materials and methods 2 2.1 Raw chemicals 2 2.2 Synthesis of Blue-TNA 2 2.3 Characterization 2 2.4 Experimental device and analytical procedures 2 3 Results and discussion 2 3.1 Morphology and structure of TNA and Blue-TNA 2 3.2 Electrochemical characterization 3 3.3 In situ generation and accumulation of PDS at anode 4 3.4 Influencing factors of PDS generation 4 3.4.1 Current density 4 3.4.2 Na2SO4concentration 4 3.4.3 Anions and dissolved oxygen 4 3.5 Mechanism of PDS generation 4 3.6 In-situ generation of PDS to degrade tetracycline 5 3.6.1 Advantages of sulfate electrochemical systems 5 3.6.2 Effects of coexisting anions and Humic acid on TC degradation 7 3.7 Blue-TNA electrode stability measurement 7 4 Conclusions 8 CRediT authorship contribution statement 8 Declaration of Competing Interest 8 Acknowledgement 8 Appendix A Supplementary data 8 References 8

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EN

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nonfiction