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In-situ monitoring of nitrate in industrial wastewater using Fourier transform infrared attenuated total reflectance spectr ... 1 1. Introduction 1 2. Experimental section 2 2.1. Wastewater sample collection 2 2.2. Chemical assay 2 2.3. Spectra determination and pretreatment 2 2.4. Prediction models 2 2.4.1. Partial least squares regression (PLSR) model 2 2.4.2. Support vector regression (SVR) model 2 2.5. Calibration and validation datasets 3 2.6. Model evaluation 3 2.7. Systematic error assessment 6 3. Results 6 3.1. Properties and characteristics of wastewater 6 3.2. FTIR-ATR spectra of industrial wastewater 6 3.3. Nitrate prediction model using original spectra 6 3.4. Spectral Gaussian deconvolution 6 3.5. Prediction model of nitrate using deconvoluted spectra 6 4. Discussion 9 4.1. Application of FTIR spectroscopy in nitrogen determination 9 4.2. Application of deconvolution in spectral data preprocessing 9 5. Conclusions 9 Declarations 10 Author contribution statement 10 Funding statement 10 Data availability statement 10 Declaration of interest’s statement 10 Additional information 10 References 10

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EN

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nonfiction