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Automatic Lab scale equipment for continuous HMF production in biphasic systems by Klushin, V A; Chizhikova, A A; Gorchakov, V V; Smirnova, N V is a Engineering article available to read on EtoBox.

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An automatic lab scale equipment for continuous HMF production by the dehydration of fructose with homogeneous catalysis in biphasic systems (water solution -MIBK) was designed, manufactured and tested. The dependencies of the HMF yield on the process parameters were studied. The feed rate of fructose varied from 50 to 100 g•h -1 , the extractant (MIBK) flow rate from 0.5 to 1.4 L•h -1 and the process temperature was maintained in the range from 50 to 87 °C. The maximum productivity of the automatic lab scale equipment 33.6 g•h -1 with a high HMF yield 48 % is achieved with the following process parameters -87 °C, the fructose feed rate 100 g•h -1 and the extractant flow rate 1 L•h -1 . This automatic lab scale equipment may be prospectively used for the kilogram scale HMF synthesis.

Who reads Automatic Lab scale equipment for continuous HMF production in biphasic systems?

Author

Klushin, V A; Chizhikova, A A; Gorchakov, V V; Smirnova, N V

Publisher

IOP Publishing (ISSN 1757-8981)

Published

2020

Language

EN

Field

Engineering (Physical Sciences)