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Optimization of the encapsulation process of Cupuassu (Theobroma grandiflorum) pulp by spray drying as an alternative for t ... 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Feed solution preparation 2 2.3 Preparation of encapsulated powders by spray drying 2 2.4 Characterization of microencapsulates 2 2.4.1 Process yield (Y) 2 2.4.2 Moisture (M) 2 2.4.3 Water activity (aw) 2 2.4.4 Water solubility index (WSI) 2 2.4.5 Hygroscopicity 2 2.4.6 Ascorbic acid encapsulation efficiency (AA) 3 2.4.7 Phenolics encapsulation efficiency (PC) 3 2.5 Experimental design and process optimization 3 2.6 Analysis of optimal microencapsulates 3 2.6.1 Scanning electron microscopy (SEM) 3 2.6.2 Bioavailability of the optimal microencapsulates under simulated digestive fluids 3 3 Results and discussion 3 3.1 Process yield 3 3.2 Moisture and water activity 5 3.3 Water solubility index (WSI) 5 3.4 Hygroscopicity 5 3.5 Ascorbic acid and phenolic encapsulation efficiency 7 3.6 Optimization 7 3.7 Powder morphology 7 3.8 Bioavailability of microcapsules under simulated digestive fluids 7 4 Conclusions 8 CRediT authorship contribution statement 8 Declaration of competing interest 8 Data avai

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EN

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nonfiction