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1 Scope 7 2 Normative references 7 3 Terms and definitions 7 4 Safety 8 5 Principle 8 5.1 Digestion 8 5.2 Determination 8 5.3 Interferences and sources of error 9 6 Apparatus 9 7 Reagents 9 8 Sample pretreatment 11 9 Alkaline digestion procedure 12 9.1 General 12 9.2 Preparation of test solutions using a hotplate or heating block 12 10 Analytical procedure 12 10.1 General information 12 10.2 Instrumental set-up 12 10.3 Calibration 13 10.4 Test solution measurement 13 10.5 Quality control 13 10.5.1 General 13 10.5.2 Blank test solution 13 10.5.3 Verification of method 13 10.5.4 Duplicate samples 14 10.5.5 Cr(VI) spiked samples 14 10.5.6 Cr(III) spiked samples 14 10.5.7 Interpretation of quality control data 14 11 Calculation 15 12 Expression of results 15 13 Test report 15

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Author

de Lerber

Language

EN

Category

reference