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Synthesis and characterization of Pd doped MXene for hydrogen production from the hydrolysis of methylamine borane: Effect of cryogenic treatment by Yaşar Karataş; Tayfun Çetin; Yuksel Akinay; Mehmet Gülcan is a Engineering article available to read on EtoBox.

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In this study, a palladium-doped cryo-MXene catalyst was prepared by a wet impregnation method and its catalytic activity was studied using the hydrolysis of methylamine-borane. The palladium nanoparticles were doped on the surface of the MXene substrate by chemical reduction of Pd +2 and characterized by different analysis techniques. The prepared palladium-doped MXene phases were cryogenically treated with liquid nitrogen at -160 • C. The morphological and structural characterization of particles was performed using a field emission scanning electron microscope, transmission electron microscope, and X-ray diffraction machine with Cu Kα radiation. The surface and bonding types of particles were determined by X-ray photoelectron spectroscopy. The palladium-doped cryo-MXene catalysts exhibited excellent catalytic performance in the hydrolysis of methylamine-borane with a turnover frequency (TOF) of 45.8 for 298 K. In addition, the palladium-doped cryo-MXene displayed good stability even after the five cycles.

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Author

Yaşar Karataş; Tayfun Çetin; Yuksel Akinay; Mehmet Gülcan

Publisher

Elsevier BV

Published

2023

Language

EN

Field

Engineering (Physical Sciences)