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Studies on Catalytic Hydrogenation of 16-Furfurylidene-17β -Hydroxy Steroids. by Milutin Stefanović; Dušan Miljković; Momčilo Miljković; Aleksandar Jokić; Božidar Stipanovic is a Chemistry article available to read on EtoBox.
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## Condensation of androstenolone (1) with furfural in the presence of sodium hydroxide under nitrogen, afforded in quantitative yield 16-furfurylidene-androstenolone (2) -m.p. 190°;C d I;"= -107~ (~~0.57 in CHCl3); UV-Spectrum:~max = 327 run (8 = 26,000); IR-Spectrum: $ max = 3509, 1724, 1640, 1563, \* 'Cyclisation of furfurylidene derivatives of cycloheianone also requires the conditions proposed by Adkins 1,2) .
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- Author
- Milutin Stefanović; Dušan Miljković; Momčilo Miljković; Aleksandar Jokić; Božidar Stipanovic
- Publisher
- Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0040-4039)
- Published
- 1966
- Language
- EN
- Field
- Chemistry (Physical Sciences)