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The azo reagent3-(5-(3-methyl-1-phenyl pyrazolazo)-1-nitroso-2-naphthol was synthesized and characterized by FT-IR ,1H-NMR and 13CNMR spectral techniques. The electrochemical behavior of the azo reagent and its complex with Fe(III) has been studied at glassy carbon disk GCE electrode in different supporting electrolyte at concentration (1M) and scan rate (100mvs-1). Spectrophotometric determination of Iron (III ) is based on the formation of a 2:1 complex with above reagent. The complex has λmax at(454) nm

Author

sunaina agarwal

Language

EN