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Synthesis of Enantiomerically Pure Cyclohex‐2‐en‐1‐ols: Development of Novel Multicomponent Reactions by Dirk Strübing; Anett Kirschner; Helfried Neumann; Sandra Hübner; Stefan Klaus; Uwe T. Bornscheuer; Matthias Beller is a Chemistry article available to read on EtoBox.
What is Synthesis of Enantiomerically Pure Cyclohex‐2‐en‐1‐ols: Development of Novel Multicomponent Reactions about?
## Abstract Multicomponent reactions of aldehydes, dienophiles, and alcohols or carboxylic acid anhydrides have been developed for the first time. In situ generation of 1‐acyloxy‐ and 1‐alkoxy‐1,3‐butadiene derivatives in toluene in the presence of electron‐deficient dienophiles provides selective and efficient access to functionalized cyclohex‐2‐ene‐1‐ols in good yields. Subsequent enzyme‐catalyzed kinetic resolution gave the corresponding enantiomers with high enantioselectivity.
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- Author
- Dirk Strübing; Anett Kirschner; Helfried Neumann; Sandra Hübner; Stefan Klaus; Uwe T. Bornscheuer; Matthias Beller
- Publisher
- John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Ltd.; Wiley (ISSN 0947-6539)
- Published
- 2005
- Language
- EN
- Field
- Chemistry (Physical Sciences)