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This study presents the synthesis of a highly active and stable layered ternary transition metal chalcogenide, Cu2MoS4, for hydrogen evolution reaction (HER). By doping with selenium, the material can be exfoliated into single-layer nanosheets, which exhibit superior electrocatalytic activity compared to multilayer forms. The single-layer TTMC maintains its structure and catalytic performance after extensive cycling, offering a promising alternative to traditional catalysts like platinum.

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