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This document discusses a novel method for the microwave-assisted cleavage of Alloc and Allyl Ester protecting groups in solid phase peptide synthesis (SPPS), which enhances the efficiency and reduces reagent usage compared to traditional methods. The new approach allows for rapid deprotection at atmospheric conditions and has been shown to achieve over 98% purity after just two 5-minute treatments at 38°C. The method was validated using various amino acid sequences, demonstrating its versatility and effect

Author

sohee.han

Language

EN