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Study of versatile coordination modes, antibacterial and radical scavenging activities of arene ruthenium, rhodium and iridium complexes containing fluorenone based thiosemicarbazones 1 1 Introduction 1 2 Experimental section 2 2.1 Physical methods and materials 2 2.2 Structure determination by single-crystal X-ray analyses 2 2.3 In vitro antimicrobial assay 2 2.4 DPPH free radical scavenging assay 2 2.5 Fluorescence studies on DNA interaction 3 2.6 General procedure for the synthesis of metal complexes (1-9) 3 2.6.1 [(p-cymene)Ru{κ2(N,S)L1(μ-S)}(μ-Cl)RuCl(p-cymene)]PF6 (1) 3 2.6.2 [Cp*Rh{κ2(N,S)L1(μ-S)}(μ-Cl)RhClCp*]PF6 (2) 3 2.6.3 [Cp*Ir(κ2(N,S)L1)Cl] (3) 5 2.6.4 [(p-cymene)Ru{κ2(N,S)L2(μ-S)}(μ-Cl)RuCl(p-cymene)]PF6 (4) 5 2.6.5 [{Cp*Rh(κ2(N,S)L2)}2](PF6)2 (5) 6 2.6.6 [Cp*Ir(κ2(N,S)L2)Cl] (6) 7 2.6.7 [(p-cymene)Ru(κ2(N,S)L3)Cl] (7) 7 2.6.8 [{Cp*Rh(κ2(N,S)L3)}2](PF6)2 (8) 7 2.6.9 [Cp*Ir(κ2(N,S)L3)Cl] (9) 7 3 Results and discussion 7 3.1 Synthesis of metal complexes 7 3.2 Spectral studies of the complexes 8 3.2.1 FT-IR studies 8 3.2.2 1H-NMR studies of complexes 8 3.2.3 13C-NMR studies of complexes 8 3.2.4 Mass studies of the complexes 8 3.2.5 UV-Visible studies of the complexes 8 3

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