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Chloride‐Promoted Photoelectrochemical C—H Silylation of Heteroarenes^†^ by Xin‐Ru Zhao; Yu‐Chen Zhang; Zhong‐Wei Hou; Lei Wang is a Chemistry article available to read on EtoBox.

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## Comprehensive Summary A photoelectrochemical approach for the C—H silylation of heteroarenes through dehydrogenation cross‐coupling with H~2~ evolution has been developed. The photoelectrochemical C—H silylation depends on hydrogen atom transfer (HAT) from silanes to Cl‐radical generated through the light‐induced homolytic cleavage of Cl~2~, in which Cl~2~ was produced by electrochemical oxidation of chloride. A large number of silylated heterocyclic molecules are rapidly constructed in satisfactory yields without relying on oxidants and metal reagents.

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Author

Xin‐Ru Zhao; Yu‐Chen Zhang; Zhong‐Wei Hou; Lei Wang

Publisher

Wiley

Published

2023

Language

EN

Field

Chemistry (Physical Sciences)