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Quantitative nuclear magnetic resonance (qNMR) is increasingly utilized for purity determination in reference material preparation, offering a more efficient alternative to traditional mass balance methods. Recent advancements include the use of heteroatoms for analysis, coupling with chromatography for improved separation, and multidimensional NMR techniques to address peak overlap issues. The development of certified reference materials (CRMs) and internal standards (IS) is crucial for achieving SI-tracea

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felipemurga

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EN