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Synthesis of magnetic NiFe2O4/CuS activator for degradation of lomefloxacin via the activation of peroxymonosulfate under s ... 1 1 Introduction 1 2 Method and material 2 2.1 Reagents 2 2.2 Fabrication of NiFe2O4/CuS 2 2.3 Characterizations 2 2.4 Degradation experiments procedure 3 3 Results and discussion 3 3.1 Characterization of NiFe2O4/CuS 3 3.1.1 SEM analysis 3 3.1.2 TEM analysis 4 3.1.3 XRD analysis 4 3.1.4 XPS analysis 4 3.1.5 VSM analysis 4 3.1.6 BET analysis 5 3.1.7 UV-DRS analysis 6 3.1.8 Photoelectrochemical property measurement 6 3.2 Evaluation of NiFe2O4/CuS photoactivators on mass ratio 6 3.3 Catalytic performance of NiFe2O4/CuS 6 3.3.1 Removal of LOM in different systems 6 3.3.2 Effect of key factor 7 3.3.3 Mineralization study 9 3.4 Reaction mechanism analysis 9 3.4.1 Free radicals’ study 9 3.4.2 Possible mechanism analysis 10 3.5 Possible degradation pathways 11 3.6 Stability and recyclability of NiFe2O4/CuS/Light/PMS reaction system 11 3.7 Leaching of metal ions 13 4 Conclusions 13 Declaration of Competing Interest 13 Acknowledgments 13 Appendix A Supplementary material 13 References 13

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Language

EN

Category

nonfiction