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New synthesis of 7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]hept-2-ene. A key intermediate in the synthesis of epibatidine and analogs by Lawrence E. Brieaddy; Feng Liang; Philip Abraham; Jeffrey R. Lee; F. Ivy Carroll is a Chemistry article available to read on EtoBox.

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A new, high yield, convenient synthesis of 7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1 ]hept-2erie which involved the addition of tributyltin hydride to 7-(tert-butoxycarbonyl)-2-p-toluenesulfonyl-7azabicyclo[2.2.1]-2-ene followed by elimination of the tributyltin and p-tolylsulfonyl groups using tetrabutylammonium fluoride was developed.

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Author

Lawrence E. Brieaddy; Feng Liang; Philip Abraham; Jeffrey R. Lee; F. Ivy Carroll

Publisher

Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0040-4039)

Published

1998

Language

EN

Field

Chemistry (Physical Sciences)