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Optimized Batchwise and Continuous Microreactor Synthesis of a (Bathophenanthroline)ruthenium(II) Complex Carrying Different Ligands by Rolf A. Kramer; Luigi Rumi; Willi Bannwarth is a Chemistry article available to read on EtoBox.

What is Optimized Batchwise and Continuous Microreactor Synthesis of a (Bathophenanthroline)ruthenium(II) Complex Carrying Different Ligands about?

## Abstract magnified image By changing the Ru‐source, the reaction conditions, and the workup/purification procedure, the batchwise synthesis of a mixed [Ru^II^(bathophenanthroline)] complex, __i.e.__, of **4b**, could substantially be improved (bathophenanthroline=4,7‐diphenyl‐1,10‐phenanthroline). In addition, we were able to adapt both steps of the synthesis to a microreactor system leading to the desired Ru‐complex in a continuous preparation in very high yields. The latter approach is especially suited for an envisaged scale‐up.

Who reads Optimized Batchwise and Continuous Microreactor Synthesis of a (Bathophenanthroline)ruthenium(II) Complex Carrying Different Ligands?

Author

Rolf A. Kramer; Luigi Rumi; Willi Bannwarth

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); Wiley-Blackwell; Wiley (ISSN 0018-019X)

Published

2009

Language

EN

Field

Chemistry (Physical Sciences)