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This research article presents the synthesis and evaluation of two-dimensional BixSby alloy nanosheets as catalysts for the electrochemical conversion of nitrogen to ammonia in neutral electrolytes. The study demonstrates that the 2D-Bi0.5Sb0.5 catalyst exhibits superior nitrogen reduction reaction performance and electrochemical stability compared to other materials, achieving a high ammonia yield and faradaic efficiency. The findings provide insights into the design of effective ternary alloy catalysts fo

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