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1. The document describes a method for the direct mechanochemical amidation of esters via ball milling. 2. The process involves ball milling an ester, amine, and sub-stoichiometric KOtBu without solvent. 3. A library of 78 amide structures was synthesized via this method in modest to excellent yields, demonstrating the scope of heteroaromatic, heterocyclic, and other functional groups tolerated.

Author

Adam

Language

EN