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Enhanced sulfate ion adsorption selectivity in capacitive deionization with ball-milled activated carbon 1 1 Introduction 2 2 Experimental section 2 2.1 Fabrication and characterization of CDI electrodes 2 2.2 Single-pass CDI experiments 2 3 Results and discussions 3 3.1 Effects of ball-milling on the physicochemical properties of CDI electrodes 3 3.1.1 Surface area and pore size distribution of ball-milled AC 3 3.1.2 Surface functional groups on ball-milled AC 3 3.1.3 Surface charge of CDI electrodes with ball-milled AC 4 3.2 Individual adsorption of Cl− and SO42− on ball-milled AC electrodes 4 3.3 Effects of pore and grain size on adsorption selectivity in Cl−/SO42− mixture 4 3.4 Effects of electrical potential distribution on adsorption selectivity in Cl−/SO42− mixture 5 3.5 Adsorption selectivity in NO3−/Cl−/SO42− mixture 7 4 Conclusions 7 CRediT authorship contribution statement 7 Declaration of competing interest 7 Data availability 8 Acknowledgements 8 Appendix A Supplementary data 8 References 8

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UND

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nonfiction