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A Low Hazard Laboratory Procedure For The Preparation of Polynitrate Esters by sirocco is a document available to read on EtoBox.
What is A Low Hazard Laboratory Procedure For The Preparation of Polynitrate Esters about?
The document presents a low hazard procedure for the laboratory preparation of polynitrate esters using a nitration method with mixed nitric-sulfuric acid and dichloromethane. This method allows for high yield and purity of the product while minimizing safety risks through careful monitoring of reaction conditions with a redox probe. The authors emphasize the importance of safety precautions and provide a detailed example of the preparation of 1-Propanediol Dinitrate.
- Author
- sirocco
- Language
- EN