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Chapter 5 Solid-Phase Synthesis Contents -1 Chapter 5 Solid-Phase Synthesis 1 5.1 THE IDEA OF SOLID- PHASE SYNTHESIS 1 5.2 SOLID- PHASE SYNTHESIS AS DEVELOPED BY MERRIFIELD 2 5.3 VESSELS AND EQUIPMENT FOR SOLID- PHASE SYNTHESIS 3 5.4 A TYPICAL PROTOCOL FOR SOLID- PHASE SYNTHESIS 5 5.5 FEATURES AND REQUIREMENTS FOR SOLID- PHASE SYNTHESIS 7 5.6 OPTIONS AND CONSIDERATIONS FOR SOLID- PHASE SYNTHESIS 8 5.7 POLYSTYRENE RESINS AND SOLVATION IN SOLID- PHASE SYNTHESIS 9 5.8 POLYDIMETHYLACRYLAMIDE RESIN 10 5.9 POLYETHYLENEGLYCOL- POLYSTYRENE GRAFT POLYMERS 12 5.10 TERMINOLOGY AND OPTIONS FOR ANCHORING THE FIRST RESIDUE 13 5.11 TYPES OF TARGET PEPTIDES AND ANCHORING LINKAGES 15 5.12 PROTECTING GROUP COMBINATIONS FOR SOLID- PHASE SYNTHESIS 16 5.13 FEATURES OF SYNTHESIS USING BOC/ BZL CHEMISTRY 16 5.14 FEATURES OF SYNTHESIS USING FMOC/ TBU CHEMISTRY 17 5.15 COUPLING REAGENTS AND METHODS FOR SOLID- PHASE SYNTHESIS 18 5.16 MERRIFIELD RESIN FOR SYNTHESIS OF PEPTIDES USING BOC/ BZL CHEMISTRY 19 5.17 PHENYLACETAMIDOMETHYL RESIN FOR SYNTHESIS OF PEPTIDES USING BOC/ BZL CHEMISTRY 20 5.18 BENZHYDRYLAMINE RESIN FOR SYNTHESIS OF PEPTIDE AMIDES USING BOC/ BZL CHEMISTRY 21 5.19 RESINS AND LINKERS FOR SYNTH

Author

N. Leo Benoiton