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Materials and Physical Measurements. All materials, reagents (including ligand) were of commercial origin and used without further purification. Microanalyses of C, H and N were determined by a CE Instruments EA 1110 elemental analyzer. The infrared spectra were recorded on a Nicolet AVATAR FT-IR IS50 spectrophotometer. Thermogravimetric analysis (TGA) curves were obtained by a SDT-Q600 thermal analyzer with a heating rate of 10 o C/min under N2 atmosphere. Powder X-ray diffraction data were recorded on a Rigaku Ultima IV powder X-ray diffractometer (Cu Kα, λ = 1.54184 Å) from 4 to 50°at room temperature. Luminescence spectra and lifetime were performed on an Edinburgh instruments FLS 980-STM apparatus, equipped with a 450 W xenon lamp. The Tb-Eu ratio was evaluated by an Agilent 7700x ICP-MS and analyzed using ICP-MS MassHunter version B01.03. Luminescence quantum yield was tested by an Edinburgh instruments FLS 1000-STM apparatus. Powder X-ray diffraction data at different temperature were recorded on a XtaLAB Synergy four-circle diffractometer with monochromatic Cu Kα radiation (λ = 1.54184 Å) from 4 to 50°. 1 H NMR spectrum was recorded on a Bruck Avance III 500MHz spectrometer

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction