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Synthesis, crystal and molecular structure and magnetic properties of [Mn(saloph)(N3)(CH3OH)] by Kou-Lin Zhang; Yan Xu; You Song; Yong Zhang; Zheng Wang; Xiao-Zeng You is a Chemistry article available to read on EtoBox.

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The mononuclear manganese(III) complex of formula [Mn(saloph)(N 3 )(CH 3 OH)] [saloph N,N 0 -o-phenylenebis(salicylidenaminato)] has been synthesized and its crystal structure has been determined by single-crystal X-ray diffraction method. The compound has a 1D hydrogen-bonded extended structure. Both the FT-IR spectrum and the electrospray ionization mass spectrum (ESI-MS) of the title compound have been recorded. The thermogravimetric analysis has also been carried out. Magnetic calculations showed the presence of antiferromagnetic exchange interactions between the manganese(III) ions through hydrogen bonds with J 24:0 cm 21 :

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Author

Kou-Lin Zhang; Yan Xu; You Song; Yong Zhang; Zheng Wang; Xiao-Zeng You

Publisher

Elsevier Science; Elsevier ; Elsevier BV (ISSN 0022-2860)

Published

2001

Language

EN

Field

Chemistry (Physical Sciences)