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Zinc nitrate hexahydrate (Zn(NO3)2•6H2O), melamine, cobalt nitrate (Co(NO3)2•6H2O), iron nitrate (Fe (NO3)2), methanol (MeOH), ethanol (C2H5OH), isopropyl alcohol (C3H8O), polyvinylpyrrolidone (PVP), zinc bis(trifluoromethanesulfonyl)imide (ZnTFSI)2, triethylamine, aniline, and Nafion were purchased from Sigma-Aldrich, USA. Potassium hydroxide (KOH), zinc acetate (Zn(OAc)2), acetonitrile, ascorbic acid, copper(II) nitrate hydrate (Cu(NO3)2•xH2O) (Daejung Chem. Korea), carbon paper (Spectra carb 2040-A, Fuel Cell Store), and Zn plate (Sigma-Aldrich, USA) were used as received. ## Fabrication of N-GC Pristine NC/GC was also prepared using a similar process without using Co(NO3)2•6H2O and acidic reactions. ## Synthesis of Pt/C Chloroplatinic acid (H2PtCl6•6H2O) with poly(N-vinyl-2-pyrrolidone) (MW = 40,000) was treated under vigorous stirring for 10 min, followed by the addition of activated carbon with continuous stirring. Furthermore, a solution of sodium borohydride (NaBH4) was transferred to the above reaction product and treated for 30 min. Finally, the Pt/C was obtained prior to centrifuging several times, washing with deionized water and then drying overnight under vacuum for 6

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Publisher

American Chemical Society (ACS)

Language

EN

Category

nonfiction