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The Photochemical 1,3-Cycloaddition of Carbonyl Compounds with Oxiranes: a Competitive Cleavage of Carboncarbon and Carbonoxygen Bonds in Ethyl 2-Methyl-3-phenylglycidate by J. Kagan; J.T. Przybytek; B.E. Firth; S.P. Singh is a Chemistry article available to read on EtoBox.

What is The Photochemical 1,3-Cycloaddition of Carbonyl Compounds with Oxiranes: a Competitive Cleavage of Carboncarbon and Carbonoxygen Bonds in Ethyl 2-Methyl-3-phenylglycidate about?

reoeived in UX for publication 13 IVovambsr 1972) When a benzene solution of either cis &-c) or trans 2-methyl-3-phenylglycidate 2-g) was irradiated in benzene under N 2 at 254 nm for 48 hrs., about 20% conversion to a complex mixture was observed. Silica gel chromatography afforded only one crystalline product m.p. 103-104: (for example, 30 mg from

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Author

J. Kagan; J.T. Przybytek; B.E. Firth; S.P. Singh

Publisher

Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0040-4039)

Published

1972

Language

EN

Field

Chemistry (Physical Sciences)