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Sustainable conversion of cottonseed hulls to valuable proanthocyanidins through ultrasound-assisted deep eutectic solvent ... 1 1 Introduction 1 2 Material and methods 2 2.1 Materials 2 2.2 Preparation and characterization of DESs 2 2.3 Extraction of PAs from CSHs 3 2.4 HPLC–MS/MS analysis 3 2.5 Determination of PAs 3 2.6 Optimization of PA extraction 3 2.7 MDS analysis 3 2.8 The difference between UAE-DES and other extraction methods 3 2.9 Determination of antioxidant activity 3 2.10 Observation of surface structure 4 2.11 Activated carbon production 4 2.12 Adsorption of MB solution 4 2.13 Statistical analysis 4 3 Results and discussion 4 3.1 Screening of DESs 4 3.2 Characterization of DESs 4 3.3 Single-factor experiments 5 3.3.1 Effect of sonication time 5 3.3.2 Effect of water content 5 3.3.3 Effect of liquid–solid ratio 5 3.4 RSM experiment 5 3.5 MDS analysis 7 3.6 The difference between UAE-DES and other extraction methods 7 3.6.1 Comparison of extraction efficiency 7 3.6.2 Comparison of antioxidant activity 9 3.6.3 HPLC–MS/MS analysis 9 3.6.4 Comparison of CSR surface morphologies 10 3.7 Characterization of biochars 10 3.8 Adsorption of biochars 10 4 Conclusion 11 Funding 1

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EN

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nonfiction