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Chiral resolution of clenbuterol, cimaterol, and mabuterol on Chirobiotic V, T, and TAG columns by Hassan Y. Aboul-Enein; Imran Ali is a Chemistry article available to read on EtoBox.

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## Chiral resolution of clenbuterol, cimaterol, and mabuterol on Chirobiotic V, T, and TAG columns The enantiomeric resolution of adrenergic b 2 -agonists (clenbuterol, cimaterol, and mabuterol) on different Chirobiotic columns (Chirobiotic V, T, and TAG) has been achieved with methanol-acetonitrile-triethylamine (80 : 20 : 0.05, v/v/v) as mobile phase. The a values of the resolved enantiomers of clenbuterol, cimaterol, and mabuterol were 1.10 to 4.26 while the values of R s varied from 1.0 to 2.10. The resolution was in the order of Chirobiotic V A Chirobiotic TAG A Chirobiotic T whereas the enantioselectivity was in the order of Chirobiotic TAG A Chirobiotic V A Chirobiotic T. The enantiomeric resolution of adrenergic b 2 -agonists on Chirobiotic columns is governed by a complex mechanism involving various types of steric interactions.

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Author

Hassan Y. Aboul-Enein; Imran Ali

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Ltd.; Wiley (ISSN 1615-9306)

Published

2002

Language

EN

Field

Chemistry (Physical Sciences)