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This research article discusses a novel method for geminal difunctionalization of ketones through the C─S bond insertion of photogenerated donor–donor diazo compounds. The study presents a metal-free process that allows for the simultaneous installation of sulfone and nitrile groups at a single carbon center, utilizing photochemical decomposition of oxadiazolines derived from ketones. The method demonstrates broad functional group tolerance, high yields, and compatibility with both batch and continuous-flow

Author

srchowdhury.chy

Language

EN