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Foreword 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Abbreviated terms 0 5 Use and classification 0 6 Sampling and repeat determinations 0 7 Determination of purity by gas chromatography (GC) 0 7.1 General 0 7.2 Interference 0 7.3 Apparatus 0 7.4 Calibration and standardization 0 7.5 Procedure 0 7.5.1 Sample preparation 0 7.5.2 Procedure A 0 7.6 Calculation 0 7.7 Precision and bias 0 7.8 Test report 0 8 Determination of purity by high-performance liquid chromatography (HPLC) 0 8.1 General 0 8.2 Apparatus 0 8.3 Reagents 0 8.4 Procedure 0 8.5 Calculation 0 8.6 Precision and bias 0 8.7 Test report 0 9 Determination of ash 0 9.1 General 0 9.2 Apparatus 0 9.3 Procedure 0 9.4 Calculation 0 9.5 Precision and bias 0 9.6 Test report 0 10 Determination of volatile matter 0 10.1 General 0 10.2 Apparatus 0 10.3 Preparation of sample 0 10.4 Procedure 0 10.5 Calculation 0 10.6 Precision and bias 0 10.7 Test report 0 Annex A (informative) Precision and bias 0 Bibliography 0

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