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Stereospecific Synthesis of 2,3-Dimethyl-1,4-thiamorpholines by Cyclization of β-N-methoxycarbonylaminoalkyl Vinyl Sulfoxides and Related Compounds by Ernesto Brunet; Maria Teresa Gallego; José Luis Garcia Ruano; Dolores Parellada; Jesús H. Rodriguez; Antonio Urbano is a Chemistry article available to read on EtoBox.
What is Stereospecific Synthesis of 2,3-Dimethyl-1,4-thiamorpholines by Cyclization of β-N-methoxycarbonylaminoalkyl Vinyl Sulfoxides and Related Compounds about?
Scheme I Preparation of starting materiah 2, 3 and 4 is outlined in Scheme II. Aziridines I-cis and X-franb were stereospecifrcally obtained in high yield from thrleoand erythro-f-methyl-Z-l~doprupyl isocyanate, reepectively, by treatment with sodium methoxide.7 Reaction of sodium 2-hydroxyethyfsulffde with atziridines 1-cis and 1-trend, followed by treatment of the resulting alcohol with thionyl chloride at OOC, yielded respectively compounds 28 and 2e.8 The structure\_s of
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- Author
- Ernesto Brunet; Maria Teresa Gallego; José Luis Garcia Ruano; Dolores Parellada; Jesús H. Rodriguez; Antonio Urbano
- Publisher
- Elsevier Science; Elsevier ; Elsevier Ltd.; Elsevier BV (ISSN 0040-4020)
- Published
- 1988
- Language
- EN
- Field
- Chemistry (Physical Sciences)