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dnced in situ by tho interaction of limo niid sodium cnrlionntc. I n this i ~n y undesirnblo subsidinry renctions, wliicli occur wlicn escess of frcc nlknli IS present, nre nvoidctl. (c) Aiiisidiiic.-'l'ho reduction of o-nitronnisol is c n r r i d out 11s ine:ins of zinc powder iind wiiter. Tho reduction procecds nioro quickly in tho prcseneo of cnlcium cliloritlo (I)ainbergcr's process), aiid discoloration niicl fornintion of di-nnisidine, such ns occur when iron nnd ligdrochloric ncid nro cniployed, nro nroidecl. Tho nitronnisol is nddcd to n solntioii of cnlciuin clilorido in tlio ninount of w t e r tlieoreticnlly rcqnired for tho retlnction, nnd tho zinc powder is slowly nddccl to tlio boiling solution. After cooling, the rcduced product is extrncted witli h i i 7 . 1 1 ~. /so\* / S I 1, ' '\OC€I, + 3%n+411,0=C I1 + 3 Z n (OIi), c 11 ' 4\ocII, (u) Ditrzotisniion and Ctrrriucol I"orniution.-llio dinzotisntion is cnsily eficcted in tho ordiiinry innnncr, tho ronction bein followed by nie:iiis of 1 4 stnrcli-iodiclo J J pnper. l!io u~iminntion of frco nitrorren and tliu fornintion of crinincol Droceed Tlio trnnsformstions offcctcd in tho production c,f vanillin from phenol mny bo

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Publisher

Wiley (John Wiley & Sons); Wiley (ISSN 0368-4075)

Published

1922

Language

EN

Field

Chemistry (Physical Sciences)