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Synthesis of Poly(spiroacetal–ether)s by Jolanta Maślińska‐Solich; Sylwia Kukowka is a Materials Science article available to read on EtoBox.

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## Abstract Poly(spiroacetal–ether)s were prepared by two alternative synthetic paths (alkaline and acid‐catalysed conditions). Polycondensation of 3,9‐di‐(2‐hydroxyphenyl)‐2,4,8,10‐tetraoxaspiro[5,5]undecane and 1,4‐dibromobutane was performed in solvents (n‐butyl acetate, __N__,__N__‐dimethylformamide, dimethyl/sulfoxide) catalysed by K~2~CO~3~ or KOH/PTC systems. A similar polymer was formed in the reaction of 2,2‐dihydroxymethyl‐1,3‐propanediol with 1,4 bis(2‐formylphenoxy)butane, catalysed by __p__‐toluenesulfonic acid. The molecular weight was determined by gel‐permeation chromatography. ^1^H and ^13^C NMR were used to study the details of the polymer structure. Copyright © 2003 Society of Chemical Industry

Who reads Synthesis of Poly(spiroacetal–ether)s?

Author

Jolanta Maślińska‐Solich; Sylwia Kukowka

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Inc.; Wiley (ISSN 0959-8103)

Published

2003

Language

EN

Field

Materials Science (Physical Sciences)