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Foreword 0 Introduction 0 1 Scope 0 2 Normative references 0 3 Terms and definitions 0 4 Symbols and abbreviated terms 0 5 Safety 0 6 Interferences 0 7 Apparatus 0 7.1 General 0 7.2 Labware 0 7.3 Drying apparatus 0 8 Reagents, standards and materials 0 9 Sample preparation 0 9.1 Environment 0 9.2 Sample 0 9.3 Specimen 0 9.4 Sample carrier 0 9.5 Trials/replicates 0 9.6 Effect of residue mass, size and its position 0 10 Procedure 0 10.1 General 0 10.2 Instrument calibration 0 10.3 Detection limit 0 10.4 TXRF measurements 0 10.5 Spectra fitting 0 10.6 Unknown samples 0 11 Qualitative and quantitative analysis 0 11.1 Identification of elements 0 11.2 Quantification of elements 0 11.3 Calculations 0 11.4 Measurement uncertainty 0 12 Quality control 0 13 Precision and accuracy 0 14 Test report 0 Annex A (informative) Uncertainty in TXRF measurements 0 Annex B (informative) Validation of the method 0 Bibliography 0

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