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Use of perbenzoic acid in analysis of unsaturated compounds. I. Preparation and stability of solutions of perbenzoic acid by I. M. Kolthoff; Thomas S. Lee; Mary Anne Mairs is a Materials Science article available to read on EtoBox.

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## Abstract The preparation of perbenzoic acid has been investigated in a n attempt to obtain standard solutions of perbenzoic acid suitable for the amlyszk of unsaturated compounds. Some modifiations of the procedure given by Braun for the preparation of a solution of perbenzoic acid in a n organic solvent are recommended. A study has been made of the stability of solutions of perbenzoic acid in chloroform and in benzene. Benzene or benzene‐chloroform mixtures are recommended as solvents for perbenzoic acid. Chloroform solutions of perbenzoic acid which do not contain inhibitors for decomposition have been found to be definitely undesirable in analytical work because perbenzoic acid catalyzes the decomposition of chloroform by oxygen. construction Finance Corporation, in connection with the Government Synthetic Rubber Program.

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Author

I. M. Kolthoff; Thomas S. Lee; Mary Anne Mairs

Publisher

John Wiley and Sons; Wiley (John Wiley & Sons); Wiley (ISSN 0022-3832)

Published

1947

Language

EN

Field

Materials Science (Physical Sciences)