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Single crystal structure features of a new Bi(III) complex, for preparation an effective bleaching catalyst 1 1 Introduction 1 2 Experimental 2 2.1 Materials 2 2.2 Synthesis of [Bi2(μ-ox)(dipic)2(H2O)2 (taa)2].H2O 2 2.3 Fabrication of β-Bi2O3 nanoparticles 2 2.4 Elemental analysis 2 2.5 ICP–AES analysis 2 2.6 EDX analysis 2 2.7 Infrared spectrum 2 2.8 Thermal characterization 2 2.9 X-ray diffraction (XRD) 2 2.10 Surface morphology 2 2.11 Measurements of surface area (BET) 2 2.12 Single crystal data collection and refinement 2 2.13 Photocatalytic experiments 2 3 Results and discussion 3 3.1 Structural studies of the Bi complex 3 3.1.1 Description of crystalline structure 3 3.1.2 FT-IR study 3 3.1.3 Thermal stability 3 3.2 Structural studies of catalyst 4 3.2.1 ICP and EDX measurements. 4 3.2.2 The XRD pattern 4 3.2.3 Scanning electron microscopy images 4 3.2.4 Textural properties 5 3.3 Photocatalytic activity 5 3.3.1 The comparison of photocatalytic activity 5 3.3.2 Mineralization and selectivity study 6 3.4 The reusability of catalyst 8 4 Conclusion 8 CRediT authorship contribution statement 9 Declaration of Competing Interest 9 Acknowledgements 9 Appendix A Supplementary data 9 Re
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Common subject areas: history, science, philosophy, social sciences.
- Language
- EN
- Category
- nonfiction
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