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Synthesis, characterization of chitosan-trithiocyanuric and its removal mechanism of Cr(VI) and Pb(II) from wastewater 1 1 Introduction 1 2 Materials and methods 2 2.1 Materials 2 2.2 Synthesis of chitosan-trithiocyanuric (CS@TMT) 2 2.2.1 Preparation of functionalized chitosan 2 2.2.2 Graft copolymerization of functionalized chitosan and trithiocyanuric acid 2 2.2.3 Determination of optimal synthesis conditions 2 2.3 Characterization 2 2.4 Methodology 2 2.4.1 Adsorption experiments 2 2.4.2 Data analysis 2 3 Results and discussion 3 3.1 Response surface optimization of CS@TMT synthesis 3 3.2 Characterization of CS@TMT 4 3.2.1 BET and SEM analysis 4 3.2.2 FTIR analysis 5 3.2.3 XRD analysis 6 3.2.4 13C NMR analysis 6 3.2.5 XPS analysis 6 3.3 Adsorption kinetics 7 3.4 Adsorption isotherms 8 3.5 Thermodynamic analysis 10 3.6 Effect of initial pH 10 3.7 Adsorption mechanism 11 3.7.1 XPS analysis before and after adsorption 11 3.8 Reusability test analysis 12 4 Conclusions 13 CRediT authorship contribution statement 15 Declaration of Competing Interest 16 Data availability 16 Acknowledgments 16 Appendix A Supplementary data 16 References 16

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EN

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nonfiction