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The document describes an efficient method for selectively synthesizing various mono-functionalized p-tert-butylcalix[4]arenes. The method involves reacting di-substituted p-tert-butylcalix[4]arenes with titanium tetrachloride to selectively remove one functional group, yielding mono-substituted derivatives. A series of mono-functionalized calixarenes were synthesized using this de-O-functionalization approach. The reaction mechanism proceeds through the formation of dioxo- and trioxo-calixarene titanium co

Author

Diogomussum

Language

EN