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Synthesis and application of [Zr-UiO-66-PDC-SO3H]Cl MOFs to the preparation of dicyanomethylene pyridines via chemical and electrochemical methods by Naseri, Amir Mohammad (author);Zarei, Mahmoud (author);Alizadeh, Saber (author);Babaee, Saeed (author);Zolfigol, Mohammad Ali (author);Nematollahi, Davood (author);Arjomandi, Jalal (author);Shi, Hu (author) is a Biochemistry, Genetics and Molecular Biology article available to read on EtoBox.
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## Abstract A metal–organic framework (MOF) with sulfonic acid tags as a novel mesoporous catalyst was synthesized. The precursor of Zr-UiO-66-PDC was synthesized both via chemical and electrochemical methods. Then, zirconium-based mesoporous metal–organic framework [Zr-UiO-66-PDC-SO~3~H]Cl was prepared by reaction of Zr-UiO-66-PDC and SO~3~HCl. The structure of [Zr-UiO-66-PDC-SO~3~H]Cl was confirmed by FT-IR, PXRD, FE-SEM, TEM, BET, EDX, and Mapping analysis. This mesoporous [Zr-UiO-66-PDC-SO~3~H]Cl was successfully applied for the synthesis of dicyanomethylene pyridine derivatives via condensation of various aldehyde, 2-aminoprop-1-ene-1,1,3-tricarbonitrile and malononitrile. At the electrochemical section, a green electrochemical method has successfully employed for rapid synthesis of the zirconium-based mesoporous metal–organic framework UiO-66-PDC at room temperature and atmospheric pressure. The synthesized UiO-66-PDC has a uniform cauliflower-like structure with a 13.5 nm mean pore diameter and 1081.6 m^2^ g^−1^ surface area. The described catalyst [Zr-UiO-66-PDC-SO~3~H]Cl was also employed for the convergent paired electrochemical synthesis of dihydropyridine derivatives as
Who reads Synthesis and application of [Zr-UiO-66-PDC-SO3H]Cl MOFs to the preparation of dicyanomethylene pyridines via chemical and electrochemical methods?
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- Author
- Naseri, Amir Mohammad (author);Zarei, Mahmoud (author);Alizadeh, Saber (author);Babaee, Saeed (author);Zolfigol, Mohammad Ali (author);Nematollahi, Davood (author);Arjomandi, Jalal (author);Shi, Hu (author)
- Publisher
- Springer Science and Business Media LLC
- Published
- 2021
- Language
- EN
- Field
- Biochemistry, Genetics and Molecular Biology (Life Sciences)