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Synthesis of Deuterated Isoflavone Disulfates by Otto Soidinsalo; Kristiina Wähälä is a Medicine article available to read on EtoBox.
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## Abstract Efficient synthesis of polydeuterated di‐__O__‐sulfates of three isoflavones, daidzein (**1**), genistein (**2**), glycitein (**3**), is described. The isoflavones were first deuterated with CF~3~COOD under microwave irradiation to yield daidzein‐__d__~6~ (**4**), genistein‐__d__~4~ (**5**) and glycitein‐__d__~6~ (**6**) in 90% yield and in a high isotopic purity. The deuterated isoflavones were then sulfated with chlorosulfonic acid and pyridine to give the title compounds, again in high yield and isotopic purity (>90%). The compounds are useful as internal standards in LC‐MS quantitation of isoflavones. Copyright © 2006 John Wiley & Sons, Ltd.
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- Author
- Otto Soidinsalo; Kristiina Wähälä
- Publisher
- John Wiley and Sons; Wiley (John Wiley & Sons); John Wiley & Sons Inc.; Wiley (ISSN 0022-2135)
- Published
- 2006
- Language
- EN
- Field
- Medicine (Life Sciences)